HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → N-[3-(2-Amino-4-methyl-phenylsulfanyl)-phenyl]-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | N-[3-(4-Methyl-2-nitro-phenylsulfanyl)-phenyl]-acetamide | HCID 68459008 | — |
| Product | N-[3-(2-Amino-4-methyl-phenylsulfanyl)-phenyl]-acetamide | HCID 68458446 | 20% |
Reaction Steps
The product from Example 71b was reduced with SnCl2 following the procedure from Example 1f providing the title compound (120 mg, 20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-9f29184c9ca4404ca000c6cfc83ee0a6 |
| Source note | uspto-grants-2012_12 |