4-Bromobenzyl bromide → 4-(4-Bromo-benzyloxy)-1-chloro-2-nitro-benzene

HRID 2197832노트

반응식

HRID 2197832 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[Br:12][C:13]1[CH:18]=[CH:17][C:16]([CH2:19]Br)=[CH:15][CH:14]=1>>[Br:12][C:13]1[CH:18]=[CH:17][C:16]([CH2:19][O:8][C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[C:3]([N+:9]([O-:11])=[O:10])[CH:4]=2)=[CH:15][CH:14]=1

참가 물질

3

반응물 2

HCID 685274-Bromobenzyl bromideHCID 691274-Chloro-3-nitrophenol

생성물 1

HCID 574698834-(4-Bromo-benzyloxy)-1-chloro-2-nitro-benzene

실험 절차

A solution of 4-chloro-3-nitro-phenol was reacted with 1-Bromo-4-bromomethyl-benzene using the conditions described in Example 237C to provide 4-(4-Bromo-benzyloxy)-1-chloro-2-nitro-benzene which was treated sequentially using the procedures from Examples 237D and 237E to provide the title product.

출처 및 근거

ORD 기록
ord-135d9aa163294105b26dd6d559efc8cb
출처 데이터셋
uspto-grants-2012_12
특허 번호
US08338605B2

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