HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 5-Bromo-2-(phenylthio)benzenamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | (4-Bromo-2-nitrophenyl)(phenyl)sulfane | HCID 14531509 | — |
| Product | 5-Bromo-2-(phenylthio)benzenamine | HCID 28401521 | 100% |
Reaction Steps
The product from Example 121b (2.0 g, 6.45 mmol) was reduced with SnCl2 following the procedure from Example 1f giving the title compound as a clear oil (1.8 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-b8f9331a2db64dbc9c19a379aaa0312c |
| Source note | uspto-grants-2012_12 |