HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,O-Dimethylhydroxylamine → 4-(4-chloro-2-nitrophenoxy)-N-methoxy-N-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,O-Dimethylhydroxylamine | HCID 14232 | — |
| Reactant | 4-(4-Chloro-2-nitrophenoxy)benzoyl chloride | HCID 86615494 | — |
| Product | 4-(4-chloro-2-nitrophenoxy)-N-methoxy-N-methylbenzamide | HCID 78776135 | 100% |
Reaction Steps
The product from Example 126c (1.0 g, 3.20 mmol) was reacted with N-methoxymethanamine (391 mg, 6.41 mmol) for 12 h following the procedure from Example 126d giving the title compound (1.03 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-62c089f53e5643a3afe4f373727ef081 |
| Source note | uspto-grants-2012_12 |