HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-nitrophenol → 4-(3-Bromo-benzyloxy)-1-chloro-2-nitro-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-nitrophenol | HCID 69127 | — |
| Reactant | 3-Bromobenzyl bromide | HCID 69979 | — |
| Product | 4-(3-Bromo-benzyloxy)-1-chloro-2-nitro-benzene | HCID 57469882 | — |
Reaction Steps
A solution of 4-chloro-3-nitro-phenol was reacted with 1-bromo-3-bromomethyl-benzene using the conditions described in Example 237C to provide 4-(3-Bromo-benzyloxy)-1-chloro-2-nitro-benzene which was treated sequentially using the procedures from Examples 237D and 237E to provide 4-[2-Amino-4-(3-bromo-benzyloxy)-phenylsulfanyl]-phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-258390ece6fc4d6b8676ad58bfc45453 |
| Source note | uspto-grants-2012_12 |