HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 68457970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 68459495 | HCID 68459495 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68457970 | HCID 68457970 | — |
Reaction Steps
The material from Example 185a (0.990 3.80 mmol) was dissolved in CH2Cl2 to which acetyl chloride (0.328 g, 4.183 mmol) was added. Reaction mixture stirred at room temperature for 1 hr at which time the title compound was collected by filtration (910 mg, 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-805ed276422b4c649b61ea4cdf39db40 |
| Source note | uspto-grants-2012_12 |