N,N-Dimethylethylenediamine → HCID 68910135, compound

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Reaction Steps

The product of Example 14 and N,N-dimethylethylenediamine were processed as in Examples 29A, 29B and 5B to afford the title compound. 1H NMR (300 MHz, CD3OD) δ ppm 0.92 (t, J=7.5 Hz, 6H), 1.54-1.72 (m, 4H), 1.80-1.89 (m, 4H), 2.19-2.30 (m, 1H), 2.36 (s, 3H), 2.64-2.78 (m, 4H), 3.00 (s, 6H), 3.38 (t, J=5.9 Hz, 2H), 3.75 (t, J=5.8 Hz, 2H), 7.21 (d, J=7.8 Hz, 2H), 7.65-7.72 (m, 2H); MS (DCI/NH3) m/z 366 (M+H)+; anal. calculated for C19H31N3O2S.C7H8O3S—H2O: C, 56.19; H, 7.44; N, 7.56. Found: C, 56.43; H, 7.61; N, 7.61.

Provenance & Evidence