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HRID2198326

反应详情

EQUATION

反应方程式

HRID 2198326 的结构方程式

REACTANTS

反应物

7
结构：C=O
HCID712

Formaldehyde

CH2O

结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：Cl.NNc1ccc(Cl)cc1
HCID71600

p-Chlorophenylhydrazine hydrochloride

C6H8Cl2N2

结构：Cl.ClCCN1CCCCC1
HCID74826

Piperidine, 1-(2-chloroethyl)-, hydrochloride

C7H15Cl2N

结构：CCOC(CCCNC)OCC
HCID13994547

4,4-Diethoxy-N-methylbutan-1-amine

C9H21NO2

结构：NN(CCN1CCCCC1)c1ccc(Cl)cc1
HCID66911628

未命名化合物

结构：CNCCc1cn(CCN2CCCCC2)c2ccc(Cl)cc12
HCID66911768

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCc2c(n(CCN3CCCCC3)c3ccc(Cl)cc23)C1
HCID44242439

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CCCC[N+](CCCC)(CCCC)CCCC.[Cl-]
催化剂HCID70681

未命名化合物

结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

The title compound was prepared by following General Methods 2, 3 and 4 using 4-chlorophenylhydrazine hydrochloride, 1-(2-chloroethyl)piperidine hydrochloride, and tetra-n-butylammonium chloride (General Method 2), 1-(4-chlorophenyl)-1-(2-(piperidin-1-yl)ethyl)hydrazine (Example 3) and 4,4-diethoxy-N-methylbutan-1-amine (General Method 3) and 2-(5-chloro-1-(2-(piperidin-1-yl)ethyl)-1H-indol-3-yl)-N-methylethanamine (Example 12), formaldehyde and TFA in acetonitrile (General Method 4).