HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tris(2-cyanoethyl)phosphine → HCID 20520070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tris(2-cyanoethyl)phosphine | HCID 77639 | — |
| Reactant | 1-Iodo-2-methoxyethane | HCID 79136 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20520070 | HCID 20520070 | — |
Reaction Steps
135.2 g (0.7 mole) of tris-(2-cyanoethyl)-phosphine are dissolved, under nitrogen, in 500 ml of boiling acetonitrile and then 130.2 g (0.7 mole) of 1-iodo-2-methoxyethane are added. The mixture is refluxed for 12 hours. After rapid filtration of the hot solution and cooling, the reaction product crystallises out and is collected by suction filtration and dried in vacuo at 60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04357280 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-7f8f318d56d141eab7ba343afa67d7a3 |
| Source note | uspto-grants-1982_11 |