Ammonium Hydroxide → 3-Methylfuran-2-carboxamide

HRID 2198425노트

반응식

HRID 2198425 반응식
[OH-].[NH4+:2].[CH3:3][C:4]1[CH:8]=[CH:7][O:6][C:5]=1[C:9](Cl)=[O:10]>>[CH3:3][C:4]1[CH:8]=[CH:7][O:6][C:5]=1[C:9]([NH2:2])=[O:10]

참가 물질

3

반응물 2

HCID 14923Ammonium HydroxideHCID 27966743-Methylfuran-2-carbonyl chloride

생성물 1

HCID 107253453-Methylfuran-2-carboxamide

실험 절차

To a stirred flask containing excess concentrated ammonium hydroxide was added gradually 50 g of 3-methyl-2-furoyl chloride. The resulting mixture was extracted with dichloromethane. The extracts were dried, then evaporated to provide solid 3-methylfuran-2-carboxamide.

후처리

  1. extractionThe resulting mixture was extracted with dichloromethane
  2. customThe extracts were dried
  3. customevaporated

출처 및 근거

ORD 기록
ord-4cb0878d1f804d99adeaa3fac0e10dce
출처 데이터셋
uspto-grants-1982_11
특허 번호
US04357345

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