HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloroquinoxaline → 4-[N-methyl-N-(3,6,7-trichloro-2-quinoxalinyl)amino]phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloroquinoxaline | HCID 16659 | — |
| Reactant | 2,3,6,7-Tetrachloroquinoxaline | HCID 4097168 | — |
| Reactant | p-(N-methylamino)phenol sulfate | HCID 10198132 | — |
| Product | 4-[N-methyl-N-(3,6,7-trichloro-2-quinoxalinyl)amino]phenol | HCID 20519115 | — |
Reaction Steps
2,3,6,7-Tetrachloroquinoxaline (mp 176° C.; prepared following essentially the same procedure as that referred to in Example 3 Part (a) for the preparation of 2,3-dichloroquinoxaline) was reacted with 4-(N-methylamino)phenol sulfate, following essentially the same procedure as that described in Example 1 Part (a), to give 4-[N-methyl-N-(3,6,7-trichloro-2-quinoxalinyl)amino]phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358307 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-76a98604540e438a8ad21624de367043 |
| Source note | uspto-grants-1982_11 |