HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-4'-methylbutyrophenone → HCID 13290821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-4'-methylbutyrophenone | HCID 98745 | — |
| Reactant | 4-Chlorobutyrophenone | HCID 253533 | — |
| Reactant | Hydrazinecarbothioamide, N-phenyl- | HCID 730679 | — |
| Reactant | Hydrazinecarbothioamide, N-2-propenyl- (9CI) | HCID 1551250 | — |
| Reactant | N-Methylhydrazinecarbothioamide | HCID 2723853 | — |
| Product | HCID 13290821 | HCID 13290821 | — |
| Product | HCID 20519427 | HCID 20519427 | — |
Reaction Steps
Analogously to the procedure of Example 1, 5,6,7,7a-tetrahydro-1-(2-propenyl-1H-pyrrolo[1,2-b][1,2,4]triazole-2(3H)-thione, 5,6,7,7a-tetrahydro-1,7a-diphenyl-1H-pyrrolo[1,2-b][1,2,4]triazole-2(3H)-thione, 7a-(4-methylphenyl)-tetrahydro-1-methyl-1H-pyrrolo[1,2-b][1,2,4]triazole-2(3H)-thione are prepared by reacting, respectively, 4-allyl-thiosemicarbazide with 1-phenyl-4-chloro-butan-1-one, 4-phenyl-thiosemicarbazide with 1-phenyl-4-chlorobutan-1-one and 4-methyl-thiosemicarbazide with 1-(4-methylphenyl)-4-chloro-butan-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358457 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-8707c808b74a4bf0a32aac24cea42882 |
| Source note | uspto-grants-1982_11 |