HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butene, 1-bromo-3-methyl- → 2-Methyl-3-(3-methyl-2-butenyl)-2-oxazolinium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Reactant | 2-Methyl-2-oxazoline | HCID 70713 | — |
| Product | 2-Methyl-3-(3-methyl-2-butenyl)-2-oxazolinium bromide | HCID 20474261 | — |
Reaction Steps
8.5 g (0.1 mol) of 2-methyloxazoline and 14.9 g (0.1 mol) of 3-methyl-2-butenyl bromide (prenyl bromide) were stirred at 20°-25° C. for 2 hours, crystalline, hygroscopic 2-methyl-3-(3-methyl-2-butenyl)-2-oxazolinium bromide being formed in an exothermic reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358598 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-e5c54eeb7cad48a9877f5ff0114258cf |
| Source note | uspto-grants-1982_11 |