HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylaniline → HCID 70546412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylaniline | HCID 6896 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | ethyl N-(2-cyano-3-ethoxyacryloyl)carbamate | HCID 230015 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70546412 | HCID 70546412 | — |
Reaction Steps
To α-cyano-β-ethoxy-N-ethoxycarbonylacrylamide (1.2 g), dissolved in about 5 ml of boiling ethanol, is added 0.6 g of 2,6-dimethylaniline. The reaction is refluxed for several hours and then hexane is added. On cooling, the reaction is filtered, and washed with ethanol and ether to give α-cyano-β-(2,6-dimethylanilino)-N-ethoxycarbonylacrylamide, m.p. 138°-140°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358591 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-29557dd00a34461fbb2dd064bcbb7f7f |
| Source note | uspto-grants-1982_11 |