HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70546412, compound → HCID 13014421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70546412 | HCID 70546412 | — |
| Solvent | P-Cymene | HCID 7463 | — |
| Product | HCID 13014421 | HCID 13014421 | — |
Reaction Steps
A mixture of α-cyano-β-(2,6-dimethylanilino)-N-ethoxycarbonylacrylamide (1.2 g) and about 10 ml of p-cymene is heated at reflux for about 1.5 hour. After cooling on standing, the crystalline product is collected by filtering and washing with ether to yield 5-cyano-1-(2,6-dimethylphenyl)uracil, m.p. 267°-269°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358591 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-4145bfac86b54157bef4b927e67f3444 |
| Source note | uspto-grants-1982_11 |