HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluoroaniline → HCID 13093903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluoroaniline | HCID 9709 | — |
| Reactant | Trichloromethanesulfenyl chloride | HCID 11666 | — |
| Reactant | HCID 2821946 | HCID 2821946 | — |
| Product | HCID 13093903 | HCID 13093903 | — |
Reaction Steps
In like manner, 5-cyano-1-(2,4-difluorophenyl)uracil is prepared, starting with 2,4-difluoroaniline, and is then reacted with trichloromethanesulfenyl chloride, giving 5-cyano-1-(2,4-difluorophenyl)-3-trichloromethanesulfenyluracil, m.p. 196°-198°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358591 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-c09c533d1c32486a89495cc32240fa7d |
| Source note | uspto-grants-1982_11 |