HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methylphenyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbonitrile → HCID 20519668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methylphenyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbonitrile | HCID 2823212 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 12806740 | HCID 12806740 | — |
| Reactant | HCID 13014421 | HCID 13014421 | — |
| Product | HCID 20519668 | HCID 20519668 | — |
| Product | HCID 20519681 | HCID 20519681 | — |
Reaction Steps
Following the procedure of Example 5, the sodium salt of 5-cyano-1-(2,6-dimethylphenyl)uracil and 5-cyano-1-(2-methylphenyl)uracil is each reacted with 2-fluoro-1,1,2,2-tetrachloroethanesulfenyl chloride to yield 5-cyano-1-(2,6-dimethylphenyl)-3-(2-fluoro-1,1,2,2-tetrachloroethanesulfenyl)uracil and 5-cyano-1-(2-methylphenyl)-3-(2-fluoro-1,1,2,2-tetrachloroethanesulfenyl)uracil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358591 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-bdedd300aef04a299196006424fbf525 |
| Source note | uspto-grants-1982_11 |