HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methylphenyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbonitrile → HCID 20519634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methylphenyl)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbonitrile | HCID 2823212 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 13014421 | HCID 13014421 | — |
| Reactant | HCID 20519645 | HCID 20519645 | — |
| Reactant | 1,1,2-Trichloro-2-(chlorosulfanyl)ethene | HCID 20519672 | — |
| Reactant | HCID 20519722 | HCID 20519722 | — |
| Product | HCID 20519634 | HCID 20519634 | — |
| Product | HCID 20519678 | HCID 20519678 | — |
| Product | HCID 20519696 | HCID 20519696 | — |
| Product | HCID 20519708 | HCID 20519708 | — |
Reaction Steps
Following the procedure of Example 5, trichloroethenesulfenyl chloride is reacted with the sodium salt of each of 5-cyano-1-(2,6-dimethylphenyl)uracil, 5-cyano-1-(2-methylphenyl)uracil, 5-cyano-1-(2-ethylphenyl)uracil and 5-cyano-1-(2,6-diethylphenyl)uracil to yield 5-cyano-1-(2,6-dimethylphenyl)-3-trichloroethenesulfenyluracil, 5-cyano-1-(2-methylphenyl)-3-trichloroethenesulfenyluracil, 5-cyano-1-(2-ethylphenyl)-3-trichloroethenesulfenyluracil and 5-cyano-1-(2,6-diethylphenyl)-3-trichloroethenesulfenyluracil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358591 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-bbf6c891cc1c45778ffc1f015aab8426 |
| Source note | uspto-grants-1982_11 |