HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloromethanesulfenyl chloride → 5-Cyano-3-trichloromethanesulfenyl-1-phenyluracil
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloromethanesulfenyl chloride | HCID 11666 | — |
| Reactant | 1,1-Dichloro-1-fluoromethanesulfenyl chloride | HCID 75926 | — |
| Reactant | 2,4-Dioxo-1-phenyl-1,2,3,4-tetrahydropyrimidine-5-carbonitrile | HCID 235105 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | 5-Cyano-3-trichloromethanesulfenyl-1-phenyluracil | HCID 20519632 | — |
Reaction Steps
The sodium salt of 5-cyano-1-phenyluracil is reacted with each of dichlorofluoromethanesulfenyl chloride and trichloromethanesulfenyl chloride following the procedure of Example 1 to yield 5-cyano-3-dichlorofluoromethanesulfenyl-1-phenyluracil and 5-cyano-3-trichloromethanesulfenyl-1-phenyluracil, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358591 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-827996e4c0044216a7627299f4bc947f |
| Source note | uspto-grants-1982_11 |