HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2198640Generated: October 30, 2026
Piperidine → 9-gamma-Piperidinopropyl-9,10-dihydro-9,10-methanoanthracene
https://huagongshe.com/reaction/2198640
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 9-gamma-Chloropropyl-9,10-dihydro-9,10-methanoanthracene | HCID 20519962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 9-gamma-Piperidinopropyl-9,10-dihydro-9,10-methanoanthracene | HCID 13069077 | — |
Reaction Steps
A mixture of 9-γ-chloropropyl-9,10-dihydro-9,10-methanoanthracene (50 mg) and piperidine (0.1 ml) was heated at 100° C. for 3 hours. The reaction mixture was diluted with ethyl acetate, washed with water, dried over anhydrous sodium sulfate and evaporated to dryness to give 9-γ-piperidinopropyl-9,10-dihydro-9,10-methanoanthracene, which was converted into its hydrochloride. M.P. 280°-283° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04358620 |
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| Source dataset | uspto-grants-1982_11 |
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| ORD ID | ord-dd8a8bd3153f4c8c9464524de81546a7 |
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| Source note | uspto-grants-1982_11 |
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