HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 9,10-Dihydro-9,10-methanoanthracene-9-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20519978 | HCID 20519978 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 9,10-Dihydro-9,10-methanoanthracene-9-carbonitrile | HCID 13069083 | — |
Reaction Steps
A solution of 9,10-dihydro-9,10-methanoanthracene-9-carboxamide (30 mg) and thionyl chloride (0.15 ml) in toluene (1 ml) was refluxed for 18 hours. Evaporation of toluene and excess thionyl chloride gave 9,10-dihydro-9,10-methanoanthracene-9-carbonitrile. M.P. 120°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358620 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-ff42026c36b149ac9b7bae73867aff3a |
| Source note | uspto-grants-1982_11 |