HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carboxin → Acetoacetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carboxin | HCID 21307 | — |
| Reactant | 2-[(2-hydroxyethyl)thio]-3-oxo-N-phenyl-butanamide | HCID 12217992 | — |
| Product | Acetoacetanilide | HCID 7592 | — |
| Product | Hydroxyethyl disulfide | HCID 15906 | — |
Reaction Steps
A method for making 5,6-dihydro-2-methyl-N-phenyl-1,4-oxathiin-3-carboxamide by cyclization of the intermediate 2-[(2-hydroxyethyl)thio]-3-oxo-N-phenyl-butanamide, in which this intermediate is obtained by the reaction of di-(2-hydroxyethyl) disulfide with acetoacetanilide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04359579 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-adffd929c89d46a28ea154025a5ec3ef |
| Source note | uspto-grants-1982_11 |