Methylamine → HCID 20517347, compound

Participants

Reaction Conditions

Reaction Steps

33.7 Parts of 2-(p-methoxybenzyloxy)-1,3-dibromo-propane, 70 parts of monomethylamine and 70 parts of water were added to an autoclave, and the mixture was heated at 90° C. for 48 hours with agitation. The reaction mixture was cooled and treated in the same manner as in Example 29, followed by distillation under reduced pressure. As a result, 11.7 parts of 3-(p-methoxybenzyloxy)-1-methylazetidine boiling at 85°-87° C. under 2 mm Hg were obtained.

Provenance & Evidence