HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)Benzaldehyde → 4-[4-(2-Chlorophenyl)-2,2-dimethyl-2,5-dihydro-1,3-oxazol-5-yl]-N,N-dimethylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Reactant | 3-(2-Chlorophenyl)-2,2-dimethyl-2H-azirene | HCID 20517776 | — |
| Product | 4-[4-(2-Chlorophenyl)-2,2-dimethyl-2,5-dihydro-1,3-oxazol-5-yl]-N,N-dimethylaniline | HCID 3061436 | — |
Reaction Steps
According to the procedure described in Example 1, from 30 g of 3-(o-chlorophenyl)-2,2-dimethyl-2H-azirine and 24 g of p-(dimethylamino)benzaldehyde there was obtained 4-(o-chlorophenyl)-5-[p-(dimethylamino)phenyl]-2,2-dimethyl-3-oxazoline which melted at 72.5°-73.5° C. after drying for 4 hours at 35° C. and 13 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360530 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-295340b0227c4833abaf214057833146 |
| Source note | uspto-grants-1982_11 |