HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20470039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Amino-1-phenylpyrazole | HCID 98736 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20470039 | HCID 20470039 | — |
Reaction Steps
A 2.0 g. amount of 3-amino-1-phenyl-2-pyrazoline (Example 1) is dissolved in 15 ml. of concentrated hydrochloric acid, then is poured into anhydrous ethyl ether to crystallize a product. The product is collected by filtration and recrystallized from acetone-hexane to give 1.50 g. of the desired product as a white solid, m.p. 94°-96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360680 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-b3e1b697470e4b05b362333f3ecb0045 |
| Source note | uspto-grants-1982_11 |