HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 54387339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 53744040 | HCID 53744040 | — |
| Product | HCID 54387339 | HCID 54387339 | — |
Reaction Steps
(3R)-6-Methylidene-5-oxo-1-thia-4-azacyclotridecane-3-carboxylic acid (0.16 g), 0.62 mmol) is dissolved in ethanol (5 ml) and hydrogen chloride gas is bubbled through the solution for 5 minutes. The solution is stirred overnight at room temperature and the solvent is evaporated to give ethyl (3R)-6-methylidene-5-oxo-1-thia-4-azacyclotridecane-3-carboxylate, m.p. 146°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426103 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-265a8ac770d84602a10c187a79d1e14e |
| Source note | uspto-grants-1995_06 |