HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzylamine hydrochloride → HCID 58433781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzylamine hydrochloride | HCID 11252467 | — |
| Reactant | HCID 21398449 | HCID 21398449 | — |
| Reactant | HCID 44462350 | HCID 44462350 | — |
| Product | HCID 58433781 | HCID 58433781 | 63% |
Reaction Steps
The named compound was synthesised from a mixture of 3-chloro-2-(4-chlorobenzoyl)benzoic acid and 6-chloro-2-(4-chlorobenzoyl)benzoic acid (2.15 g, 7.28 mmol) and 4-nitrobenzylamine hydrochloride (1.51 g, 8.01 mmol) using General Procedure B, purified by chromatography (Biotage SP4; 10%-20% EtOAc/petrol) and obtained as a white solid (1.96 g, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09358222B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-a1a44354e3c24d6abd9cfd14bbf4b60f |
| Source note | uspto-grants-2016_06 |