HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzylamine hydrochloride → HCID 44595607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzylamine hydrochloride | HCID 11252467 | — |
| Reactant | HCID 58433799 | HCID 58433799 | — |
| Product | HCID 44595607 | HCID 44595607 | 44.4% |
Reaction Steps
The named compound was synthesised from 2-(4-chlorobenzoyl)cyclohex-1-enecarboxylic acid (1.00 g, 3.78 mmol) and 4-nitrobenzylamine hydrochloride (0.78 g, 4.16 mmol) using General Procedure B, purified by chromatography (Biotage SP4; 30% EtOAc/petrol) and obtained as a yellow solid (0.67 g, 44%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09358222B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-10c3855533e4402db1be1faefeac9b3d |
| Source note | uspto-grants-2016_06 |