5-Formylbenzene-1,2,3-triyl triacetate → HCID 117664734, compound

Participants

Reaction Steps

Use diethyl 3,5-dimethoxybenzyl phosphate and 3,4,5-triacetoxybenzaldehyde as materials, and follow the method described in Example 5 to obtain a white solid as the target product (75%). 1H NMR (400 MHz, DMSO-d6): 2.08 (s, 9H), 3.77 (s, 6H), 6.22 (s, 1H), 6.84 (s, 2H), 6.91 (d, J=16.0 Hz, 1H), 6.92 (d, J=16.0 Hz, 1H), 7.01 (s, 2H).

Provenance & Evidence