Potassium Hydroxide → HCID 89914271, compound

HRID 2199960Notes

Reaction equation

HRID 2199960 reaction equation
[CH3:1][C:2]1[CH:22]=[CH:21][CH:20]=[C:19]([CH3:23])[C:3]=1[CH2:4][N:5]1[C:13]2[C:8](=[CH:9][CH:10]=[C:11]([CH2:14][C:15]([OH:17])=[O:16])[CH:12]=2)[C:7]([CH3:18])=[CH:6]1.[OH-].[K+:25]>C(O)C>[CH3:1][C:2]1[CH:22]=[CH:21][CH:20]=[C:19]([CH3:23])[C:3]=1[CH2:4][N:5]1[C:13]2[C:8](=[CH:9][CH:10]=[C:11]([CH2:14][C:15]([O-:17])=[O:16])[CH:12]=2)[C:7]([CH3:18])=[CH:6]1.[K+:25]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 60152007HCID 60152007, compound

Product 1

HCID 89914271HCID 89914271, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of the compound [64] (226 mg) in ethanol (5 mL) was added an aqueous solution of 1N-potassium hydroxide (0.74 mL) at room temperature, and the solution was concentrated under reduced pressure to give the titled compound (254 mg) as a yellow solid.

Workup

  1. concentrationthe solution was concentrated under reduced pressure

Sources & evidence

ORD record
ord-aba5445dbdf8471baa851762bcc7af86
Source dataset
uspto-grants-2016_06
Patent number
US09359350B2

Reaction notes

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