HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylvinyltin → tert-butyl 2,3-dihydro-6-vinyl-1H-indole-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylvinyltin | HCID 81998 | — |
| Reactant | tert-Butyl 6-bromoindoline-1-carboxylate | HCID 22038386 | — |
| Reactant | 1-(2,6-dimethylbenzyl)-1H-indole-6-carboxylic acid | HCID 68184345 | — |
| Product | tert-butyl 2,3-dihydro-6-vinyl-1H-indole-1-carboxylate | HCID 86707256 | — |
Reaction Steps
The titled compound (207 mg) as a white solid was prepared from tert-butyl 6-bromo-2,3-dihydro-1H-indole-1-carboxylate obtained by the method described in the document (WO 1998/43956 A) and tributyl(vinyl)tin according to the method of the process (2) of Example 66.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359350B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-b9ff2b227a3942cc95f0e759da3722af |
| Source note | uspto-grants-2016_06 |