HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → potassium 2-[1-(2,6-dichlorobenzyl)-3-methyl-1H-indazole-6-yl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 60152151 | HCID 60152151 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | potassium 2-[1-(2,6-dichlorobenzyl)-3-methyl-1H-indazole-6-yl]acetate | HCID 131732622 | — |
Reaction Steps
To a solution of the compound [97] (118 mg) in ethanol (5 mL) was added an aqueous solution of 1N-potassium hydroxide (0.34 mL) at room temperature, and then the reaction mixture was stirred at room temperature for 10 minutes. The reaction mixture was concentrated under reduced pressure to give the titled compound (128 mg) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359350B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-7c38aebe47d747a289d277ba92082e0d |
| Source note | uspto-grants-2016_06 |