化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Carbonate → Pteridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | Diisopropylethylamine | HCID 81531 | — |
| 反応物 | 2-Chloropteridine | HCID 640537 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | Pteridine | HCID 1043 | — |
反応手順
Treatment of chloro-pteridine V′ with nuclephile R7LY, in the presence of a base, such as sodium hydride, potassium carbonate, triethylamine, and diisopropylethylamine, and optionally using a catalyst such as Pd(0), affords Pteridine compound VI′. Suitable solvent for this reaction includes chloroform, methylene chloride, toluene, and tetrahydrofuran.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09359361B2 |
| 出典データセット | uspto-grants-2016_06 |
| ORD ID | ord-d9c56d6283074992ae1b8b6cf1b5d281 |
| 出典メモ | uspto-grants-2016_06 |