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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2200325Generated: October 31, 2026

Sulfuric Acid → HCID 86672600, compound

https://huagongshe.com/reaction/2200325

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfuric AcidHCID 1118—
ReactantMilademetanHCID 73297272—
SolventIsopropanolHCID 3776—
ProductHCID 86672600HCID 8667260062.9%

Reaction Steps

Concentrated sulfuric acid (0.005 ml, 0.08 mmol) was added to a 2-propanol (0.5 ml) solution of the compound (52 mg, 0.08 mmol) obtained in Example 1 and then the resulting mixture was stirred at room temperature for 2 days. The precipitate was collected by filtration to give 20 mg (34%) of the title compound as a solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09359368B2
Source datasetuspto-grants-2016_06
ORD IDord-cc38a4e34bd246939f5d9fcd2bda8983
Source noteuspto-grants-2016_06