HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 86672600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Milademetan | HCID 73297272 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86672600 | HCID 86672600 | 62.9% |
Reaction Steps
Concentrated sulfuric acid (0.005 ml, 0.08 mmol) was added to a 2-propanol (0.5 ml) solution of the compound (52 mg, 0.08 mmol) obtained in Example 1 and then the resulting mixture was stirred at room temperature for 2 days. The precipitate was collected by filtration to give 20 mg (34%) of the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359368B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-cc38a4e34bd246939f5d9fcd2bda8983 |
| Source note | uspto-grants-2016_06 |