HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → Methyl 2-(4-(benzyloxy)-3-bromophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 2-(3-bromo-4-hydroxyphenyl)acetate | HCID 10634081 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Methyl 2-(4-(benzyloxy)-3-bromophenyl)acetate | HCID 56605342 | — |
Reaction Steps
Compound 10 (12.3 g) was dissolved in 100 mL acetone and 7.6 g of potassium carbonate was added. 8.6 g of benzyl bromide was added with stirring. The solid was removed by suction filtration and the liquid was evaporated to product 11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359372B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-d183db3ee6454f69b0c850e9b2968b79 |
| Source note | uspto-grants-2016_06 |