HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetone → HCID 90402786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | 1181458-10-5 | HCID 21105142 | — |
| Product | HCID 90402786 | HCID 90402786 | — |
Reaction Steps
A solution of 3-(cyanomethyl)benzamide (200 mg, 1.25 mmol) in 1-chloropropan-2-one (2 mL) was microwave irradiated at 120 for 20 min in a sealed tube. The mixture was concentrated to give crude product (110 mg), which was directly used to the next reaction without purification. LCMS MH+ 199.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359359B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-a67079d97cd44a5fa76841c3a5d6db89 |
| Source note | uspto-grants-2016_06 |