HuagongsheHuagongshe Chemistry Print Report · For research reference only
Erucic Acid → Docos-13-EN-1-YL octadec-9-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Erucic Acid | HCID 5281116 | — |
| Reactant | Oleoyl chloride | HCID 5364783 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | Docos-13-EN-1-YL octadec-9-enoate | HCID 54339620 | 94.5% |
Reaction Steps
Compound D was prepared from Oleoyl chloride and Erucic acid following the general procedure discussed before and as shown in FIG. 9. Pure compound D was a colorless oil obtained by column chromatography with Ethyl acetate/Hexane=1:40. Reaction conditions for branched derivative compounds D2, D3, and D4 are also shown below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359571B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-9462af5039834b0983732a222f302fc4 |
| Source note | uspto-grants-2016_06 |