9-Decen-1-ol → Dec-9-enyl dec-9-enoate

HRID 2201163Notes

Reaction equation

HRID 2201163 reaction equation
[CH2:1]([OH:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10].[C:12](O)(=[O:22])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH:20]=[CH2:21]>C(OCC)(=O)C.CCCCCC>[C:1]([O:22][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH:20]=[CH2:21])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10]

Participants

4

Reactant 2

HCID 256129-Decen-1-olHCID 617439-Decenoic acid

Product 1

HCID 86669122Dec-9-enyl dec-9-enoateYield 92.7%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Compound G was prepared from 9-decen-1-ol and 9-decenoic acid following the general procedure already discussed and shown in FIG. 12. Pure compound G was a colorless oil by column chromatography with Ethyl acetate/Hexane=1:50.

Sources & evidence

ORD record
ord-5083d18732bb49e5bb2f736bcc16d9f8
Source dataset
uspto-grants-2016_06
Patent number
US09359571B2

Reaction notes

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