Dimethyl Carbonate → HCID 67399232, compound

HRID 2201601Notes

Reaction equation

[OH-].[C:2]12([N+:12]([CH3:15])([CH3:14])[CH3:13])[CH2:11][CH:6]3[CH2:7][CH:8]([CH2:10][CH:4]([CH2:5]3)[CH2:3]1)[CH2:9]2.C12(N(C)C)CC3CC(CC(C3)C1)C2.[C:29](=[O:34])([O:32]C)[O:30][CH3:31]>>[CH3:31][O:30][C:29](=[O:32])[O-:34].[C:2]12([N+:12]([CH3:15])([CH3:14])[CH3:13])[CH2:9][CH:8]3[CH2:7][CH:6]([CH2:5][CH:4]([CH2:10]3)[CH2:3]1)[CH2:11]2

Participants

Reactant 3

HCID 12021Dimethyl Carbonate

HCID 19478N,N-Dimethyl-1-adamantanamine

HCID 14475644N,N,N-Trimethyl-1-adamantylammonium hydroxide

Product 1

HCID 67399232HCID 67399232, compound

Procedure

The invention is a method for preparing 1-adamantyltrimethylammonium hydroxide. The method comprises reacting 1-adamantyldimethylamine with dimethyl carbonate to produce 1-adamantyltrimethylammonium methylcarbonate, which is then reacted with calcium hydroxide or magnesium hydroxide in the presence of water to produce 1-adamantyltrimethylammonium hydroxide.

Sources & evidence

ORD record: ord-82f3d4b8974d4fe5abcda2cbe1d6fb0b
Source dataset: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09365490B2

Reaction notes

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