Dimethyl Carbonate → HCID 67399232, compound

HRID 2201602Notes

Reaction equation

[C:1]12([N:11]([CH3:13])[CH3:12])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[C:14](=[O:19])([O:17]C)[O:15][CH3:16]>>[CH3:16][O:15][C:14](=[O:17])[O-:19].[C:1]12([N+:11]([CH3:14])([CH3:13])[CH3:12])[CH2:8][CH:7]3[CH2:6][CH:5]([CH2:4][CH:3]([CH2:9]3)[CH2:2]1)[CH2:10]2

Participants

Reactant 2

HCID 12021Dimethyl Carbonate

HCID 19478N,N-Dimethyl-1-adamantanamine

Product 1

HCID 67399232HCID 67399232, compound

Procedure

The method of the invention comprises reacting 1-adamantyldimethylamine with dimethyl carbonate to produce 1-adamantyltrimethylammonium methylcarbonate. The 1-adamantyltrimethylammonium methylcarbonate is then reacted with calcium hydroxide or magnesium hydroxide in the presence of water to produce 1-adamantyltrimethylammonium hydroxide

Sources & evidence

ORD record: ord-8f690bd9c1214245bb86d5e1553b8f7c
Source dataset: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09365490B2

Reaction notes

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