HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic Acid → HCID 66613436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic Acid | HCID 1110 | — |
| Reactant | Lorcaserin | HCID 11658860 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Isopropyl Acetate | HCID 7915 | — |
| Product | HCID 66613436 | HCID 66613436 | — |
Reaction Steps
The title salt was prepared by the addition of succinic acid (0.5-1 eq.) in hot EtOH to a solution of (R)-8-chloro-1-methyl-2,3,4,5-tetrahydro-1H-3-benzazepine in isopropyl acetate. After overnight stirring, a solid was recovered by suction filtration and washed in isopropyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365521B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-33c1d145489e471b837d239579ef4d5d |
| Source note | uspto-grants-2016_06 |