HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90149137, compound → HCID 90149563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90149137 | HCID 90149137 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 90149563 | HCID 90149563 | — |
Reaction Steps
A3 was dissolved in EtOAc/MeOH (1:1) (0.01 M) and treated with Pd/C. Mixture was purged with N2 and stirred under H2 atmosphere at room temperature for 24 h. Then, reaction mixture was filtered through a pad of silica and filtrate was concentrated under vacuum to give the title compound which was used as such in the next step. MS (ES+) C21H27N5O2: 382 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365541B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-e25e61f9ebd0482cb5cafde6548dc773 |
| Source note | uspto-grants-2016_06 |