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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2202544Generated: November 1, 2026

HCID 90149137, compound → HCID 90149563, compound

https://huagongshe.com/reaction/2202544

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 90149137HCID 90149137—
CatalystPalladiumHCID 23938—
SolventEthylacetate methanolHCID 21584119—
ProductHCID 90149563HCID 90149563—

Reaction Steps

A3 was dissolved in EtOAc/MeOH (1:1) (0.01 M) and treated with Pd/C. Mixture was purged with N2 and stirred under H2 atmosphere at room temperature for 24 h. Then, reaction mixture was filtered through a pad of silica and filtrate was concentrated under vacuum to give the title compound which was used as such in the next step. MS (ES+) C21H27N5O2: 382 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09365541B2
Source datasetuspto-grants-2016_06
ORD IDord-e25e61f9ebd0482cb5cafde6548dc773
Source noteuspto-grants-2016_06