HCID 90149152, compound → HCID 90149567, compound

Participants

Reaction Steps

E3 was dissolved in EtOAc/MeOH (1:1, 0.1 M) and treated with Pd/C (10% w/w). Mixture was purged with N2 and stirred under H2 atmosphere at room temperature for 16 h. Then, reaction mixture was filtered through a pad of Solka-Floc® and filtrate was concentrated under reduced pressure to give the title compound as pale yellow oil which was used as such in the next step. MS (ES+) C22H28N4O2: 381 (M+H)+.

Provenance & Evidence