HCID 68877689, compound → HCID 86684824, compound

Participants

Reaction Steps

3-Chloro-4′-hydroxy-3′,4′,5′,6′-tetrahydro-2′H-[2,4′]bipyridinyl-1′-carboxylic acid tert-butyl ester (0.18 g) was dissolved in a solution of hydrogen chloride in dioxane (4 N, 2 mL). The mixture was stirred for 0.5 hours and the solvent removed by evaporation under vacuum. The solid was triturated from ether to afford the title compound (0.15 g). LCMS m/z 213.1 [M+H]+. R.T.=0.79 min (Analytical Method 3).

Provenance & Evidence