Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 56776714 | HCID 56776714 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 68775670 | HCID 68775670 | — |
Reaction Steps
2-Chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzo[d]imidazole (200 mg, 0.718 mmol) and aniline (669 mg, 7.18 mmol) were mixed in N-methyl-2-pyrrolidinone (2 mL). The solution was heated at 140° C. for 30 minutes in a microwave reactor. The reaction mixture was concentrated to give the title compound, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09365566B2 |
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| Source dataset | uspto-grants-2016_06 |
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| ORD ID | ord-06fce8eaec974ae9977cc432d572cc8a |
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| Source note | uspto-grants-2016_06 |
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