Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2203232Generated: October 30, 2026

Aniline → HCID 68775670, compound

https://huagongshe.com/reaction/2203232

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAnilineHCID 6115—
ReactantHCID 56776714HCID 56776714—
SolventN-methyl-2-pyrrolidoneHCID 13387—
ProductHCID 68775670HCID 68775670—

Reaction Conditions

Temperature140 °C

Reaction Steps

2-Chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzo[d]imidazole (200 mg, 0.718 mmol) and aniline (669 mg, 7.18 mmol) were mixed in N-methyl-2-pyrrolidinone (2 mL). The solution was heated at 140° C. for 30 minutes in a microwave reactor. The reaction mixture was concentrated to give the title compound, which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09365566B2
Source datasetuspto-grants-2016_06
ORD IDord-06fce8eaec974ae9977cc432d572cc8a
Source noteuspto-grants-2016_06