HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-bromo-1-methyl-1H-imidazo(4,5-b)pyridine → 4-amino-7-methyl-8-(1-methyl-1H-imidazo[4,5-b]pyridin-6-yl)cinnoline-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-bromo-1-methyl-1H-imidazo(4,5-b)pyridine | HCID 10856781 | — |
| Reactant | 4-Amino-8-bromo-7-methylcinnoline-3-carboxamide | HCID 89825213 | — |
| Product | 4-amino-7-methyl-8-(1-methyl-1H-imidazo[4,5-b]pyridin-6-yl)cinnoline-3-carboxamide | HCID 89833439 | — |
Reaction Steps
The title compound was prepared in a manner similar to EXAMPLE 96 using 6-bromo-1-methyl-1H-imidazo[4,5-b]pyridine and 4-amino-8-bromo-7-methylcinnoline-3-carboxamide. 1H NMR (400 MHz, CD3OD) δ ppm 2.37 (s, 3 H), 3.98 (s, 3 H), 7.76 (d, J=9.09 Hz, 1 H), 8.09 (d, J=1.77 Hz, 1 H), 8.29 (d, J=8.59 Hz, 1 H), 8.39 (d, J=2.02 Hz, 1H), 8.47 (s, 1 H); ESI-MS m/z [M+H]+ 334.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365566B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-6c9e79d2febc4a78b523717f97f530cf |
| Source note | uspto-grants-2016_06 |