HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-[1,2,4]triazolo[4,3-a]pyridine → 8-([1,2,4]Triazolo[4,3-a]pyridin-6-yl)-4-amino-7-methylcinnoline-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-[1,2,4]triazolo[4,3-a]pyridine | HCID 17750018 | — |
| Reactant | 4-Amino-8-bromo-7-methylcinnoline-3-carboxamide | HCID 89825213 | — |
| Product | 8-([1,2,4]Triazolo[4,3-a]pyridin-6-yl)-4-amino-7-methylcinnoline-3-carboxamide | HCID 89826696 | — |
Reaction Steps
The title compound was prepared in a manner similar to EXAMPLE 96 using 6-bromo-[1,2,4]triazolo[4,3-a]pyridine and 4-amino-8-bromo-7-methylcinnoline-3-carboxamide. 1H NMR (400 MHz, CD3OD) δ ppm 2.45 (s, 3 H), 7.45 (d, J=9.35 Hz, 1 H), 7.78 (d, J=8.84 Hz, 1 H), 7.92 (d, J=9.60 Hz, 1 H), 8.34 (d, J=8.84 Hz, 1 H), 8.56 (s, 1 H), 9.25 (s, 1 H); ESI-MS m/z [M+H]+ 320.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365566B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-38da3f492d554c3d8d32c02e2968cb77 |
| Source note | uspto-grants-2016_06 |