HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Bromoimidazo(1,5-a)pyridine → 4-Amino-8-(imidazo[1,5-a]pyridin-7-yl)-7-methylcinnoline-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Bromoimidazo(1,5-a)pyridine | HCID 66888640 | — |
| Reactant | 4-Amino-8-bromo-7-methylcinnoline-3-carboxamide | HCID 89825213 | — |
| Product | 4-Amino-8-(imidazo[1,5-a]pyridin-7-yl)-7-methylcinnoline-3-carboxamide | HCID 89826643 | — |
Reaction Steps
The title compound was prepared in a manner similar to EXAMPLE 96 using 7-bromoimidazo[1,5-a]pyridine and 4-amino-8-bromo-7-methylcinnoline-3-carboxamide. 1H NMR (400 MHz, CD3OD) δ ppm 2.44 (s, 3 H), 6.64 (dd, J=7.07, 1.52 Hz, 1 H), 7.44 (s, 1 H), 7.50 (s, 1 H), 7.71 (d, J=8.59 Hz, 1 H), 8.23 (d, J=8.84 Hz, 1 H), 8.35 (d, J=7.07 Hz, 1 H), 8.42 (s, 1 H); ESI-MS m/z [M+H]+ 319.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365566B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-c398e2c0e5c6420ba9ba2c67411eb96a |
| Source note | uspto-grants-2016_06 |