HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxybenzeneacetonitrile → (2Z)-2-(3,4-dimethoxyphenyl)-3-{4-[(8-hydroxyoctyl)oxy]phenyl}prop-2-enenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| Reactant | 4-[(8-Hydroxyoctyl)oxy]benzaldehyde | HCID 86725128 | — |
| Product | (2Z)-2-(3,4-dimethoxyphenyl)-3-{4-[(8-hydroxyoctyl)oxy]phenyl}prop-2-enenitrile | HCID 71272357 | 46% |
Reaction Steps
(2Z)-2-(3,4-dimethoxyphenyl)-3-{4-[(8-hydroxyoctyl)oxy]phenyl}prop-2-enenitrile is prepared starting from 4-[(8-hydroxyoctyl)oxy]benzaldehyde and the commercial (3,4-dimethoxyphenyl)acetonitrile according the same procedure following for example 1 in 46% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-fee935e73d5b438cb5b6bcf572c24c9c |
| Source note | uspto-grants-2016_06 |