HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-(Methylenedioxy)phenylacetonitrile → HCID 71272566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-(Methylenedioxy)phenylacetonitrile | HCID 78178 | — |
| Reactant | 4-[(11-Hydroxyundecyl)oxy]benzaldehyde | HCID 14965977 | — |
| Product | HCID 71272566 | HCID 71272566 | 73% |
Reaction Steps
(2Z)-2-(1,3-benzodioxol-5-yl)-3-{4-[(11-hydroxyundecyl)oxy]phenyl}prop-2-enenitrile is prepared starting from 4-[(11-hydroxyundecyl)oxy]benzaldehyde and commercial [3,4-(methylenedioxy)phenyl]acetonitrile according the same procedure following for example 1 in 73% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-eeccb24abb714c25bbd3ceb12ffd13d9 |
| Source note | uspto-grants-2016_06 |